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Changes in the structure and properties of ZrO2 detonation coatings during annealing

https://doi.org/10.29317/ejpfm.2020040405

Abstract

The article studied the effect of annealing on the structure and properties of zirconium dioxide coatings obtained by detonation spraying. Detonation spraying was realized on a computerized detonation spray ing complex of the new generation CCDS2000. Determined that coatings made of zirconium dioxide are characterized by high adhesive strength of adherence to the substrate. Thermal annealing of coated samples was performed at temperatures of 900-1200C. It was determined that the microhardness of zir conium dioxide coatings increases by 10-25% depending on the annealing temperature after annealing. The results of nanoindentation showed that the nanohardness of the coatings after annealing at 1000C increases by 50%. It was determined that after annealing at 1000C, the elastic modulus of the coatings increases, which indicates a decrease in plasticity and an increase in the strength of the coatings. X-ray diffraction analysis showed that the phase composition of coatings before and after annealing consists of t-ZrO2. After annealing occurs there is an increase in the degree of t-ZrO2 tetragonality. Electron microscopic analysis showed that an increase in the number and size of micro-continuity in the form of thin layers after annealing. Determined that increase the hardness of zirconium dioxide after annealing at 900-1200C is associated with a higher degree of tetragonality t-ZrO2 phase.

About the Authors

B. K. Rakhadilov
Sarsen Amanzholov East Kazakhstan University; PlasmaScience LLP
Kazakhstan


D. N. Kakimzhanov
Sarsen Amanzholov East Kazakhstan University; D. Serikbayev East Kazakhstan Technical University;
Kazakhstan


G. .. Botabaeva
Sarsen Amanzholov East Kazakhstan University
Kazakhstan


D. B. Buitkenov
Sarsen Amanzholov East Kazakhstan University; PlasmaScience LLP
Kazakhstan


N. .. Kantai
Sarsen Amanzholov East Kazakhstan University; D. Serikbayev East Kazakhstan Technical University;
Kazakhstan


L. B. Bayatanova
PlasmaScience LLP
Kazakhstan


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Review

For citations:


Rakhadilov B.K., Kakimzhanov D.N., Botabaeva G..., Buitkenov D.B., Kantai N..., Bayatanova L.B. Changes in the structure and properties of ZrO2 detonation coatings during annealing. Eurasian Journal of Physics and Functional Materials. 2020;4(4):319-326. https://doi.org/10.29317/ejpfm.2020040405

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ISSN 2522-9869 (Print)
ISSN 2616-8537 (Online)